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INTERNATIONAL JOURNAL OF NOVEL RESEARCH AND DEVELOPMENT International Peer Reviewed & Refereed Journals, Open Access Journal ISSN Approved Journal No: 2456-4184 | Impact factor: 8.76 | ESTD Year: 2016 Scholarly open access journals, Peer-reviewed, and Refereed Journals, Impact factor 8.76 (Calculate by google scholar and Semantic Scholar | AI-Powered Research Tool) , Multidisciplinary, Monthly, Indexing in all major database & Metadata, Citation Generator, Digital Object Identifier(DOI) |
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| Paper Title: | DEVLOPMENT AND VALIDATION OF RP-HPLC METHOD FOR QUANTIFICATION OF THIOCOLCHICOSIDE AND DCLOFENAC DIETHYLAMINE IN PRESENCE OF ACTIVE EXCIPIENTS FROM THEIR COMBINED SEMISOLID TOPICAL PREPARATION |
| Authors Name: | LOHIYA NISHABEN NARESHBHAI , MR KETAN RATHOD , DR CHAITANYA BHATT , DR. VANITA MARVANIYA |
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IJNRD_197165
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| Published Paper Id: | IJNRD2305798 |
| Published In: | Volume 8 Issue 5, May-2023 |
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| Abstract: | A simple, accurate, precise, specific reverse phase high performace liquid chromatography method was developed and validated for quantification of Thiocolchicoside and Diclofenac Diethylamine in combined pharmaceutical formulation (gel). The approach was validated for Thiocolchicoside and Diclofenac Diethylamine using ICH recommendations over a range of 1-5 µg/mL and 9-45 µg/mL for Thiocolchicoside and Diclofenac Diethylamine respectively. An analytical column HYPERSIL ODS C18, 250 mm*4.6 mm was utilized. At a flow rate of 1.0 ml/min, the mobile phase was Acetonitrile and 0.025M potassium hydrogen phosphate buffer in a (50:50 v/v) ratio. The elution was examined using a UV detector with a detection wavelength of 254 nm. The retention times for Thiocolchicoside and Diclofenac Diethylamine are 4.3 minutes and 9.8 minutes, respectively. The percentage recoveries for Thiocolchicoside and Diclofenac Diethylamine were 99.00-101.5 % and 99.11-100.22 %, respectively. The RSD values are not greater than 2%. |
| Keywords: | Thiocolchicoside, Diclofenac Diethylamine, RP-HPLC Method |
| Cite Article: | "DEVLOPMENT AND VALIDATION OF RP-HPLC METHOD FOR QUANTIFICATION OF THIOCOLCHICOSIDE AND DCLOFENAC DIETHYLAMINE IN PRESENCE OF ACTIVE EXCIPIENTS FROM THEIR COMBINED SEMISOLID TOPICAL PREPARATION", International Journal of Novel Research and Development (www.ijnrd.org), ISSN:2456-4184, Vol.8, Issue 5, page no.h769-h787, May-2023, Available :http://www.ijnrd.org/papers/IJNRD2305798.pdf |
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2456-4184 | IMPACT FACTOR: 8.76 Calculated By Google Scholar| ESTD YEAR: 2016 An International Scholarly Open Access Journal, Peer-Reviewed, Refereed Journal Impact Factor 8.76 Calculate by Google Scholar and Semantic Scholar | AI-Powered Research Tool, Multidisciplinary, Monthly, Multilanguage Journal Indexing in All Major Database & Metadata, Citation Generator |
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Published Paper ID:IJNRD2305798 Registration ID: 197165 Published In: Volume 8 Issue 5, May-2023 DOI (Digital Object Identifier): Page No: h769-h787 Country: AHEMEDABAD, GUJRAT, INDIA Research Area: Pharmacy Publisher : IJ Publication Published Paper URL : https://www.ijnrd.org/viewpaperforall?paper=IJNRD2305798 Published Paper PDF: https://www.ijnrd.org/papers/IJNRD2305798 |
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ISSN: 2456-4184
Impact Factor: 8.76 and ISSN APPROVED
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